Separation of Gold, Palladium and Platinum from Metallurgical Samples Using an Amberlite XAD-7 Resin Column Prior to Their Atomic Absorption Spectrometric Determinations

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Separation of gold, palladium and platinum from metallurgical samples using an amberlite XAD-7 resin column prior to their atomic absorption spectrometric determinations.

A simple and sensitive method for the separation and preconcentration of gold, palladium and platinum has been established prior to their atomic absorption spectrometric determinations. Analytes from 0.5 mol dm(-3) KI in a 2 mol dm(-3) HCl solution were recovered using an Amberlite XAD-7 column as halogeno complexes. The effects of some analytical parameters, including reagent amounts, sample v...

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Preconcentration of lead with Amberlite XAD-2 and Amberlite XAD-7 based chelating resins for its determination by flame atomic absorption spectrometry.

Four chelating matrices prepared by coupling Amberlite XAD-2 with chromotropic acid (AXAD-2-CA or 1), pyrocatechol (AXAD-2-PC or 2) and thiosalicylic acid (AXAD-2-TSA or 3) through azo spacer and impregnation of Amberlite XAD-7 with xylenol orange (AXAD-7-XO or 4) have been studied for enrichment of lead(II). All the four resins quantitatively sorb Pb(II) at pH 3.0-8.0 when the flow rate is mai...

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Comparison of Modified Palladium Nanoparticles and Homemade Activated Carbon Derived from Medlar for Solid Phase Extraction of Metal Ions Prior to Their Flame Atomic Absorption Spectrometry Determination

This study focus on the preparation of two supports including activated carbon derived from medlar and Palladium nanoparticles loaded on activated carbon (Pd-NP-AC). Subsequently, both adsorbent modified with a novel Schiff base chelating agent and their potential applicability for determination of trace amounts of metal ions from aqueous solution has been investigated. The method is based on c...

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Adsorption characteristics of as(III) and as(V) with titanium dioxide loaded Amberlite XAD-7 resin.

The adsorption characteristics of As(V) and As(III) on titanium dioxide loaded Amberlite XAD-7 resin have been studied. The resin was prepared by impregnation of Ti(OC2H5)4 followed by hydrolysis with ammonium hydroxide. Batch adsorption experiments were carried out as a function of the pH, shaking time and the concentration of As(V) and As(III) ions. The resin showed a strong adsorption for As...

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Removal of Acid-soluble Lignin from Biomass Extracts Using Amberlite Xad-4 Resin

This paper describes a method for the removal of acid-soluble lignin from acid-hydrolyzed hemicelluloses extracted from a mixture of northern US hardwood chips, by using Amberlite XAD-4 resin, which was shown to remove 100% of furan derivatives and 90% of acid-soluble lignin. Subsequent fermentation of the resin-treated hydrolyzates gave ethanol yields as high as 97% of theoretical and showed a...

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ژورنال

عنوان ژورنال: Analytical Sciences

سال: 2003

ISSN: 0910-6340,1348-2246

DOI: 10.2116/analsci.19.1621